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18:34 Jul 17, 2017
English to Russian translations [PRO]
Tech/Engineering - Chemistry; Chem Sci/Eng / Хроматография
English term or phrase: CV
The mixtures were allowed to stir at RT for 2 hours at which time LC-MS showed completed conversion. Quenched with 10ml 1N HCl. The mixtures were poured into 250ml of EtOAc, washed with 10% LiCl twice, Brine once. The organic layer was then dried over Na2SO4 and concentrated. The crude materials were purified by RediSep Column: Silica 220g
Flow Rate: 150 ml/min
Equilibration Volume: 1.0 ***CV***
Solvent: A1 hexane; Solvent: B1 ethyl acetate
Gradient 0%--40% Sol B in 15mins.
Fractions containing the desired product were combined and dried via centrifugal evaporation to provide the title compound (1.86g, 65%).
Analysis LCMS Condition A: Retention time = 1.14 min; ESI-MS(+) m/z 477.1 (M+H).
Vorontsova
Russian Federation
Local time: 07:48
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Summary of answers provided
3 +5объем колонкиMarzena Malakhova


  

Answers


2 mins   confidence: Answerer confidence 3/5Answerer confidence 3/5 peer agreement (net): +5
cv
объем колонки


Explanation:
column volume

Marzena Malakhova
Russian Federation
Local time: 07:48
Native speaker of: Native in RussianRussian
PRO pts in category: 8

Peer comments on this answer (and responses from the answerer)
agree  Leila Usmanova
6 mins
  -> Спасибо, Лейла!

agree  Natalie
20 mins
  -> Спасибо, Наталья!

agree  Tatiana Nikitina
1 hr
  -> Спасибо, Татьяна!

agree  Erzsébet Czopyk
13 hrs
  -> Спасибо!

agree  svetlana cosquéric
1 day19 hrs
  -> Спасибо, Светлана!
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