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02:26 Aug 6, 2004
This question was closed without grading. Reason: No acceptable answer
English to Chinese translations [PRO] Medical - Chemistry; Chem Sci/Eng
English term or phrase:Dess-Martin Periodinane
Step 1. To a solution of 2-(1-tert-butoxycarbonyl-1H-thieno[3,2-c]pyrazol-3-yl)-5-(hydroxy-phenyl-methyl)-indole-1-carboxylic acid tert-butyl ester [640mg, 1.l7 mmol, Intermediate (12)] in Dichloromethane (25 mL) is added Dess-Martin Periodinane (677 mg, 1.69 mmol) and stirred at room temperature.
步骤1. 向2 - ( 1 -叔丁氧羰基- 1H -噻吩併[ 3,2 - c]吡唑- 3 -基- 5 - (羟-苯基甲基) -吲哚-羧酸叔丁基酯[ 640mg, 1.l7 mmol,中间体( 12)]的二氯甲烷( 25 mL)溶液中加入Dess - Martin Periodinane ( 677 mg 1.69 mmol),在室温下搅拌。