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16:55 Dec 20, 2016
This question was closed without grading. Reason: Errant question
English to Russian translations [PRO] Science - Medical: Pharmaceuticals / лиофилизация
English term or phrase:the resistance to the sublimating water
Due to the large fill volume, it is necessary to set the shelf temperature considerably warmer than the glass transition temperature in order to compensate for evaporative cooling. The solution temperature during primary drying was at -29°C, which is near the glass transition temperature of -28°C from the DSC thermal analysis.
The reduced fill volume minimizes the competing evaporative cooling of the surrounding vials and minimizes ***the resistance to the sublimating water***.